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Beilstein J. Org. Chem. 2024, 20, 661–671, doi:10.3762/bjoc.20.59
Graphical Abstract
Scheme 1: Background (a and b) and proposed carboamination MCR with diazo esters (c). a) Selected bioactive γ...
Scheme 2: Substrate scope of diazo compounds, 1,3-dienes and amines. aReactions (1/2/3/Pd(OAc)2/Xantphos = 0....
Scheme 3: Substrate scope of diazo compounds, allenes and amines. aReactions (1/5/3/Pd(OAc)2/Xantphos = 0.3.0...
Scheme 4: Mechanistic experiments. a) Radical trapping experiments with TEMPO. b) Exclusion of possible inter...
Scheme 5: Proposed mechanisms for the carboamination of 1,3-dienes or allenes with diazo esters and amines.
Scheme 6: Scale-up reactions and synthetic transformations. Reaction conditions: a) LiAlH4, THF, 0 °C; b) MeM...
Beilstein J. Org. Chem. 2014, 10, 746–751, doi:10.3762/bjoc.10.69
Scheme 1: Previous work for (R)-(1-amino-3-methylbutyl)boronic acid synthesis.
Scheme 2: Synthesis of (R)-4 and Velcade.
Figure 1: ORTEP diagram of (S,S,R)-3a (left, most of the hydrogen atoms were omitted except the one on the ch...
Scheme 3: Synthesis of phosphinylimines and their borylation products.